ࡱ> %` bjbjNN 8,,%vvvvvvv0008&11S2B4B4"d4d4d4?5?5?5VSXSXSXSXSXSXS$ UhqW|Sv 8?5?5 8 8|Svvd4d4S=== 80vd4vd4VS= 8VS==rHTvvId464 PX0P9vZH JL S0ShHW9WIWvI?55h=96T6?5?5?5|S|SN=j?5?5?5S 8 8 8 8d,00vvvvvv  PACN GC-MS WORKSHOP PROGRAMME JOMO KENYATTA UNIVERSITY OF AGRICULTURE AND TECHNOLOGY DEPARTMENT OF CHEMISTRY 2nd - 6th MARCH, 2009 DAY 1: MONDAY 2nd MARCH, 2009 OPENING CEREMONY: Venue: Lecture Theatre (ACC100) Chair: Prof S. Chacha Master of ceremony: Dr Tsanuo, M.K. (Chairman, 91AV Department - JKUAT)TIMEEVENTPRESENTERS8.30 - 9.00(a) Arrival & Registration of ParticipantsSecretariat9.00 - 9.45(b) Remarks:- CoD 91AVDr Tsanuo, M.K. - Dean, Faculty of ScienceProf Mulati D. - Chair PACN KenyaProf WandigaS.O. -DCV (RPE)Prof Kahangi E. -DVC (APD)Prof Njeru F. -DVC (AA)Prof Odhiambo R.9.45 - 10.15Official Opening & Opening remarksProf Imbuga M.10.15 - 10.45Tea BreakTRAINING SESSION 1 Venue: IEET ENV LAB10.45 - 11.30GC Instrumentation:Prof. Antony Gachanja/ Dr. Steve Lancaster(a) Gas chromatography-basic theory``(b) Columns and separation considerations``(c) Injection systems``11.30 - 12.30Mass Spectrometer instrumentation:``(a)Basic Theory``(b) Ionization``(c) Mass spectrometer types``12.30 - 1.00Open Discussion1.00 - 2.00Lunch BreakTRAINING SESSION 2 Venue: IEET ENV LAB2.00 - 3.30Practical Session 1: IEET ENV LAB/GC-MS LABBasic Maintenance for GC-MSProf. Antony Gachanja/ Dr. Steve Lancaster3.30 - 4.0Tea break4.00 - 5.00Basic Maintenance for GC-MS (Contd)``5.30 7.00COCKTAIL Venue: AICAD Sponsored by: PACN Kenya DAY 2: TUESDAY 3rd MARCH, 2009 TRAINING SESSION 3 Venue: IEET ENV LAB8.30 - 10.00Basic Spectral interpretation:(a) IntroductionProf. Antony Gachanja/ Dr. Steve Lancaster(b) Isotope abundances how can these be useful?``(c) Spectral appearance including some examples``10.00 - 10.30Tea Break10.30 - 12.30Elemental formulas including ``(a) isotopic abundances,``(b) use of abundances for determining carbon and oxygen, rings plus double bonds equivalents``12.30 - 1.00Open Discussion1.00 - 2.00Lunch BreakTRAINING SESSION 4 Venue: IEET ENV LAB2.00 - 3.30Practical Session 2: Exercises to determine simple structuresProf. Antony Gachanja/ Dr. Steve Lancaster3.30 - 4.00Tea break4.00 - 5.00Exercises to determine simple structures (Contd)`` DAY 3: WEDNESDAY 4TH MARCH, 2009 TRAINING SESSION 5 Venue: IEET ENV LAB8.30 - 10.00More advanced methods in spectral interpretation includingProf. Antony Gachanja/ Dr. Steve Lancaster(a) Nitrogen rule``(b) Molecular ion ``(c) Molecular weight determination``10.00 - 10.30Tea break10.30 - 12.30Single bond cleavage``Multiple bond cleavage``Rearrangements, specifically McLafferty``12.30 - 1.00Open Discussion1.00 - 2.00Lunch BreakTRAINING SESSION 6 Venue: IEET ENV LAB2.00 - 3.30Exercises in spectral interpretation``3.30 - 4.00Tea break 4.00 - 5.00Exercises in spectral interpretation (Contd)`` DAY 4: THURSDAY 4TH MARCH, 2009 TRAINING SESSION 7 Venue: GC-MS LAB8.30 - 10.00Practical session 3Setting up and tuning the mass spectrometerProf. Antony Gachanja/ Dr. Steve Lancaster10.00 - 10.30Tea break10.30 - 1.00Setting up and tuning the mass spectrometer (Contd)``1.00 - 2.00Lunch break2.00 - 3.30Quantitative exercises including the use of internal standards``3.30 - 4.00Tea break4.00 - 5.00Quantitative exercises including the use of internal standards (Contd)`` DAY 5: FRIDAY 5TH MARCH 2009 TRAINING SESSION 8 Venue: IEET ENV LAB8.30 - 10.00Sample pre-treatment includingProf. Antony Gachanja/ Dr. Steve Lancaster- solid phase extraction``- liquid/liquid extraction``Identification of unknowns in an analgesic drug sample``Designing experiments to quantify some compounds in the above matrix``10.00 - 10.30Tea Break10.30 - 11.30Open Discussion11.30 - 1.00Way forward1.00 - 2.30Lunch Break2.30 - 3.30Closing Ceremony     PAGE  PAGE 1   U`mnoqtuwx   * 2 3 4 < R S W X Y Z _ ¾ œ ¾ ¾¾¾ hhCJaJhhh4BCJaJh+VhFh hhP-j5h4BhP-jhIm5hP-jh4B5H*hwhP-jhP-jhY"s5hP-jhY"s5H*hP-jhw5 hw 5hP-jh065hP-jh4B5 hw5 h54Vn; $Ifgdw $IfgdP-jgd4B$a$gdw$a$gd06 ; < A G R ypg $Ifgd $Ifgd06 $$Ifa$gd hzkd$$Iflt""  t 0"644 lap ytGR S _ ne\S $IfgdrK $Ifgd06 $Ifgdhkd$$IflFnPt"$ t0"6    44 layth_ c m y     " # $ % 8 9 E Q T U V W i j w ۽۽h+VCJaJh hhrKCJaJhhhP-jCJaJhhCJaJhhh4BCJaJh4Bh hhP-jCJaJh hh4BCJaJG ne\S $Ifgd $Ifgd06 $IfgdhkdO$$IflFnPt"$ t0"6    44 layth neXO $Ifgd $If^gd h $Ifgdhkd$$IflFnPt"$ t0"6    44 layth  # neXO $IfgdrK $If^gd h $Ifgdhkd$$IflFnPt"$ t0"6    44 layth# $ % E U ne\S $Ifgd+V $Ifgd06 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